2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

Base Information

Chemical Name:2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide
CAS No.:1296820-97-7
Molecular Formula:C₂₂H₂₁NO₅S₂
Molecular Weight:443.544
Hs Code.:

Synonyms:2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

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Chemical Property of 2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

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Technology Process of 2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

There total 3 articles about 2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1296820-80-8
2-hydroxynaphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

: 157668-05-8
(1-bromo-pent-4-enyl)-benzene

: 1296820-97-7
2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 16h;
DOI:10.1039/c0ob00976h

Reference yield:

: 57821-65-5
naphtho<1,8-cd>-1,2-dithiole 1,1,2-trioxide

: 1296820-97-7
2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 20 °C

2: potassium carbonate / acetone / 16 h / 20 °C

With hydrogenchloride; potassium carbonate; sodium nitrite; In 1,4-dioxane; water; acetone;
DOI:10.1039/c0ob00976h

Reference yield:

: 40227-43-8
naphtho<1,8-cd>-1,2-dithiole 1,1-dioxide

: 1296820-97-7
2-(1-phenylhex-5-en-1-yloxy)naphtho[1,8-de][1,3,2]dithiazine 1,1,3,3-tetraoxide

Guidance literature:: Multi-step reaction with 3 steps

1: urea hydrogen peroxide adduct; sodium hydroxide / 1,4-dioxane; water / 0.25 h

2: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 20 °C

3: potassium carbonate / acetone / 16 h / 20 °C

With hydrogenchloride; urea hydrogen peroxide adduct; potassium carbonate; sodium hydroxide; sodium nitrite; In 1,4-dioxane; water; acetone;
DOI:10.1039/c0ob00976h