Technology Process of C59H86(2)H6O4
There total 7 articles about C59H86(2)H6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 24 h / Ambient temperature
2: sodium iodide, trimethylsilyl chloride / acetonitrile / 50 °C
3: potassium carbonate / acetone / 4 h / 50 °C
4: aq. KOH / CHCl3; methanol
5: sodium hydrosulphite / diethyl ether / 0.03 h
6: boron trifluoride etherate / dioxane / Ambient temperature
With
pyridine; potassium hydroxide; sodium disulfite; chloro-trimethyl-silane; boron trifluoride diethyl etherate; potassium carbonate; sodium iodide;
In
1,4-dioxane; methanol; diethyl ether; chloroform; acetone; acetonitrile;
DOI:10.1016/S0040-4039(00)61251-0
- Guidance literature:
-
Multi-step reaction with 7 steps
1: aq. sodium hydrosulphite / diethyl ether / 0.03 h
2: pyridine / 24 h / Ambient temperature
3: sodium iodide, trimethylsilyl chloride / acetonitrile / 50 °C
4: potassium carbonate / acetone / 4 h / 50 °C
5: aq. KOH / CHCl3; methanol
6: sodium hydrosulphite / diethyl ether / 0.03 h
7: boron trifluoride etherate / dioxane / Ambient temperature
With
pyridine; potassium hydroxide; sodium disulfite; chloro-trimethyl-silane; boron trifluoride diethyl etherate; potassium carbonate; sodium iodide;
In
1,4-dioxane; methanol; diethyl ether; chloroform; acetone; acetonitrile;
DOI:10.1016/S0040-4039(00)61251-0
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrosulphite / diethyl ether / 0.03 h
2: boron trifluoride etherate / dioxane / Ambient temperature
With
sodium disulfite; boron trifluoride diethyl etherate;
In
1,4-dioxane; diethyl ether;
DOI:10.1016/S0040-4039(00)61251-0