Technology Process of C29H30N2O5
There total 8 articles about C29H30N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
5-{[(E)-methoxyimino]phenylmethyl}-1H-indole;
With
sodium hydride;
In
mineral oil;
at 0 - 20 ℃;
Inert atmosphere;
2-(S)-3-[4-(2-chloroethoxy)-phenyl]-2-ethoxypropionic acid;
In
mineral oil;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/cmdc.201200316
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen; palladium 10% on activated carbon / ethanol / 20 h / 20 °C / 760.05 Torr
2.1: lithium hydroxide / water; tetrahydrofuran / 20 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0 - 20 °C
4.1: sulfuric acid / water; 1,4-dioxane / 8 h / Reflux
5.1: sodium hydride / mineral oil / 0 - 20 °C / Inert atmosphere
5.2: 12 h / 20 °C / Inert atmosphere
With
sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; mineral oil;
DOI:10.1002/cmdc.201200316
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide / water; tetrahydrofuran / 20 h / 20 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0 - 20 °C
3.1: sulfuric acid / water; 1,4-dioxane / 8 h / Reflux
4.1: sodium hydride / mineral oil / 0 - 20 °C / Inert atmosphere
4.2: 12 h / 20 °C / Inert atmosphere
With
sulfuric acid; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; mineral oil;
DOI:10.1002/cmdc.201200316