C₂HF₃O₂*C₂₄H₂₇N₇O₅S

Base Information

Chemical Name:C₂HF₃O₂*C₂₄H₂₇N₇O₅S
CAS No.:1354542-63-4
Molecular Formula:C₂HF₃O₂*C₂₄H₂₇N₇O₅S
Molecular Weight:639.612
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>24</sub>H<sub>27</sub>N<sub>7</sub>O<sub>5</sub>S

Synonyms:C₂HF₃O₂*C₂₄H₂₇N₇O₅S

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Chemical Property of C₂HF₃O₂*C₂₄H₂₇N₇O₅S

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Technology Process of C₂HF₃O₂*C₂₄H₂₇N₇O₅S

There total 5 articles about C₂HF₃O₂*C₂₄H₂₇N₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354542-50-9
C₃₇H₄₄N₇O₈S⁽¹⁺⁾*I^(1-)

: 76-05-1
trifluoroacetic acid

: 1354542-63-4
C₂HF₃O₂*C₂₄H₂₇N₇O₅S

Guidance literature:: With methyl-phenyl-thioether; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1021/ja208290f

Reference yield:

: para-methoxybenzyl (6R,7R)-7-amino-3-chloromethyl-3-cephem-4-carboxylate hydrochloride

: 1354542-63-4
C₂HF₃O₂*C₂₄H₂₇N₇O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 3 h / 0 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / acetone / 0.25 h / 0 °C

3: sodium iodide / acetone / 1 h / 20 °C

4: acetonitrile / 6 h / 20 °C / Inert atmosphere

5: methyl-phenyl-thioether / dichloromethane / 4 h / 0 °C

With methyl-phenyl-thioether; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja208290f

Reference yield:

: C₂₄H₃₀IN₃O₈S

: 1354542-63-4
C₂HF₃O₂*C₂₄H₂₇N₇O₅S

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 6 h / 20 °C / Inert atmosphere

2: methyl-phenyl-thioether / dichloromethane / 4 h / 0 °C

With methyl-phenyl-thioether; In dichloromethane; acetonitrile;
DOI:10.1021/ja208290f