C₂₁H₂₇NO₄

Base Information

Chemical Name:C₂₁H₂₇NO₄
CAS No.:1402573-63-0
Molecular Formula:C₂₁H₂₇NO₄
Molecular Weight:357.45
Hs Code.:

C<sub>21</sub>H<sub>27</sub>NO<sub>4</sub>

Synonyms:C₂₁H₂₇NO₄

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Chemical Property of C₂₁H₂₇NO₄

Chemical Property:

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Technology Process of C₂₁H₂₇NO₄

There total 7 articles about C₂₁H₂₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1402573-62-9
C₂₁H₂₇N₃O₄

: 1402573-63-0
C₂₁H₂₇NO₄

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201203379

Reference yield:

: 110-89-4
piperidine

: 1402573-63-0
C₂₁H₂₇NO₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: trimethylaluminum / hexane; dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: acetic acid / methanol; water / 0.17 h / 20 °C

3.2: 2 h / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 48 h / 0 °C / Inert atmosphere

5.1: water / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

7.1: N,N’-bistosylhydrazine / toluene / 5 h / 100 °C / Inert atmosphere

7.2: 12 h / 20 °C / Inert atmosphere

8.1: silver trifluoromethanesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; N,N’-bistosylhydrazine; water; trimethylaluminum; silver trifluoromethanesulfonate; Dess-Martin periodane; acetic acid; dimethyl sulfoxide; In 1,4-dioxane; methanol; hexane; dichloromethane; water; toluene;
DOI:10.1002/anie.201203379

Reference yield:

: 1402573-61-8
C₂₁H₂₇NO₅

: 1402573-63-0
C₂₁H₂₇NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N’-bistosylhydrazine / toluene / 5 h / 100 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: silver trifluoromethanesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

With N,N’-bistosylhydrazine; silver trifluoromethanesulfonate; In dichloromethane; toluene;
DOI:10.1002/anie.201203379