2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Base Information

• Chemical Name: 2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol
• CAS No.: 850428-42-1
• Molecular Formula: C₇₄H₇₉N₃O₁₅
• Molecular Weight: 1250.45

Synonyms:2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Chemical Property of 2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Chemical Property:

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Technology Process of 2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

There total 1 articles about 2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,2R,3S,4S,5R,6S)-3-{(2R,3R,4R,5S,6R)-3-Azido-4-benzyloxy-6-benzyloxymethyl-5-[(2R,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-2-yloxy]-tetrahydro-pyran-2-yloxy}-4,5,6-tris-benzyloxy-cyclohexane-1,2-diol → 2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol (850428-42-1)

Guidance literature:

With sodium methylate; In methanol; for 0.166667h;

DOI:10.1039/b418041k

Reference yield: 100.0%

2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol (850428-42-1) → α-D-mannopyranosyl-(1->4)-2-ammonio-2-deoxy-α-D-glucopyranosyl-(1->6)-D-myo-inositol

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 12h;

DOI:10.1039/b418041k

Reference yield: 95.0%

2,3,4-tri-O-benzyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol (850428-42-1) + triisopropylsilyl chloride (13154-24-0) → 2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:

With 1H-imidazole; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 10h;

DOI:10.1081/CAR-200066956

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