4-(benzylamino)-α-oxophenylacetic acid

Base Information

Chemical Name:4-(benzylamino)-α-oxophenylacetic acid
CAS No.:75626-71-0
Molecular Formula:C₁₅H₁₃NO₃
Molecular Weight:255.273
Hs Code.:

Synonyms:4-(benzylamino)-α-oxophenylacetic acid

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Chemical Property of 4-(benzylamino)-α-oxophenylacetic acid

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Technology Process of 4-(benzylamino)-α-oxophenylacetic acid

There total 6 articles about 4-(benzylamino)-α-oxophenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75626-69-6
methyl 4-(benzylamino)-α-oxophenylacetate dimethyl ketal

: 75626-71-0
4-(benzylamino)-α-oxophenylacetic acid

Guidance literature:: With lithium iodide; In pyridine; at 90 ℃; for 5h;
DOI:10.1021/jo00314a029

Reference yield:

: 73549-48-1
4-acetamido-α-oxophenylacetic acid

: 75626-71-0
4-(benzylamino)-α-oxophenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 98percent H₂SO₄ / 48 h

2: 1.) acetic acid, 2.) sodium cyanoborohydride / 1.) ethanol, 15 min, 2.) 30 min

3: 100 percent / lithium iodiide / pyridine / 5 h / 90 °C

With sulfuric acid; sodium cyanoborohydride; acetic acid; lithium iodide; In pyridine;
DOI:10.1021/jo00314a029

Reference yield:

: 75626-41-4
methyl 4-amino-α-oxophenylacetate dimethyl ketal

: 75626-71-0
4-(benzylamino)-α-oxophenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) acetic acid, 2.) sodium cyanoborohydride / 1.) ethanol, 15 min, 2.) 30 min

2: 100 percent / lithium iodiide / pyridine / 5 h / 90 °C

With sodium cyanoborohydride; acetic acid; lithium iodide; In pyridine;
DOI:10.1021/jo00314a029