(1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

Base Information

Chemical Name:(1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester
CAS No.:1107648-86-1
Molecular Formula:C₁₇H₂₇NO₃
Molecular Weight:293.406
Hs Code.:

Synonyms:(1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

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Chemical Property of (1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

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Technology Process of (1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

There total 3 articles about (1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1107648-85-0
(1R,3S)-(-)-3-(1-allylamino-1-methylethyl)cyclohexanecarboxylic acid methyl ester

: 814-68-6,25189-84-8
acryloyl chloride

: 1107648-86-1
(1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmcl.2010.01.139

Reference yield:

: 1107648-81-6
C₁₁H₂₁NO₂

: 1107648-86-1
(1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetonitrile

2: triethylamine / dichloromethane

With sodium hydrogencarbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.001

Reference yield:

: 1107648-80-5
(1R,3S)-(-)-3-(1-methyl-1-nitroethyl)cyclohexanecarboxylic acid methyl ester

: 1107648-86-1
(1R,3S)-(-)-3-[1-(N-acryloyl-N-allylamino)-1-methylethyl]cyclohexanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen hexachloroplatinate; hydrogen / methanol

2: sodium hydrogencarbonate / acetonitrile

3: triethylamine / dichloromethane

With dihydrogen hexachloroplatinate; hydrogen; sodium hydrogencarbonate; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.001