(3R,3aR,3a¹S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a¹,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline

Base Information

• Chemical Name: (3R,3aR,3a¹S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a¹,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline
• CAS No.: 942622-33-5
• Molecular Formula: C₂₁H₂₇NO₂
• Molecular Weight: 325.451

Synonyms:(3R,3aR,3a¹S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a¹,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline

Chemical Property of (3R,3aR,3a¹S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a¹,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline

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Technology Process of (3R,3aR,3a¹S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a¹,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline

There total 2 articles about (3R,3aR,3a¹S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a¹,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-((3R,3aR,3a1S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-2,3,3a,4,7,8-hexahydro-3a1H-benzo[de]quinolin-1(6aH)-yl)-2,2,2-trifluoroethanone → (3R,3aR,3a1S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a1,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline (942622-33-5)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 5h;

DOI:10.1002/anie.200605160

Reference yield:

(S)-6-((4E,6E)-7-(3,5-dimethoxyphenyl)hepta-4,6-dienyl)-4-methoxy-3-methyl-2,3,4,5-tetrahydropyridine → (3R,3aR,3a1S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a1,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline (942622-33-5)

Guidance literature:

With trifluoroacetic acid; In tetrahydrofuran; water; at 50 ℃; for 18h;

DOI:10.1002/anie.200605160

Reference yield:

(3R,3aR,3a1S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-3,3a,3a1,4,6a,7,8,9-octahydro-2H-benzo[de]quinoline (942622-33-5) + trifluoroacetic anhydride (407-25-0) → 1-((3R,3aR,3a1S,4S,6aR)-4-(3,5-dimethoxyphenyl)-3-methyl-2,3,3a,4,7,8-hexahydro-3a1H-benzo[de]quinolin-1(6aH)-yl)-2,2,2-trifluoroethanone

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/anie.200605160

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