C₅₅H₈₂O₁₄Si

Base Information

Chemical Name:C₅₅H₈₂O₁₄Si
CAS No.:215876-30-5
Molecular Formula:C₅₅H₈₂O₁₄Si
Molecular Weight:995.333
Hs Code.:

C<sub>55</sub>H<sub>82</sub>O<sub>14</sub>Si

Synonyms:C₅₅H₈₂O₁₄Si

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Chemical Property of C₅₅H₈₂O₁₄Si

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Technology Process of C₅₅H₈₂O₁₄Si

There total 8 articles about C₅₅H₈₂O₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 247146-69-6
C₅₅H₈₄O₁₄Si

: 215876-30-5
C₅₅H₈₂O₁₄Si

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane;
DOI:10.1021/ja990860j

Reference yield:

: 215876-26-9
C₅₆H₇₈O₁₅

: 215876-30-5
C₅₅H₈₂O₁₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / DMAP / CH₂Cl₂ / 10 °C

2: 62 percent / 1,4-cyclohexadiene / 10 percent Pd/C / ethyl acetate

3: i-PrNEt₂ / benzene

4: 81 percent / DMAP / benzene

5: PPTS; HC(OCH₃)3 / methanol; CH₂Cl₂ / -30 °C

6: 66 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂

With pyridine; dmap; N,N-diethyl-N-isopropylamine; cyclohexa-1,4-diene; pyridinium p-toluenesulfonate; Dess-Martin periodane; trimethyl orthoformate; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate; benzene; 1: silylation / 2: debenzylation / 3: Esterification / 4: Cyclization / 5: desilylation / 6: Oxidation;
DOI:10.1021/ja990860j

Reference yield:

: 215876-25-8
C₇₉H₁₃₂O₁₅Si₄

: 215876-30-5
C₅₅H₈₂O₁₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: HF*pyr; pyridine / tetrahydrofuran / 72 h

2: 65 percent / DMAP / CH₂Cl₂ / 10 °C

3: 62 percent / 1,4-cyclohexadiene / 10 percent Pd/C / ethyl acetate

4: i-PrNEt₂ / benzene

5: 81 percent / DMAP / benzene

6: PPTS; HC(OCH₃)3 / methanol; CH₂Cl₂ / -30 °C

7: 66 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂

With pyridine; dmap; N,N-diethyl-N-isopropylamine; cyclohexa-1,4-diene; pyridinium p-toluenesulfonate; Dess-Martin periodane; pyridine hydrogenfluoride; trimethyl orthoformate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; benzene; 1: Cyclization / 2: silylation / 3: debenzylation / 4: Esterification / 5: Cyclization / 6: desilylation / 7: Oxidation;
DOI:10.1021/ja990860j