<3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

Base Information

Chemical Name:<3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone
CAS No.:135501-76-7
Molecular Formula:C₂₃H₃₃NO₅
Molecular Weight:403.519
Hs Code.:

Synonyms:<3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

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Technology Process of <3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

There total 1 articles about <3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 135396-80-4
(4S)-3-<(2R,3S,4S)-(E)-2-ethyl-3-hydroxy-4,6-dimethyl-1-oxonon-6-enyl>-4-methyl-5-phenyl-2-oxazolidinone

: 135501-76-7
<3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

: 135396-82-6
(4R,5S)-3-{(R)-2-[(2S,3S,5R)-5-((S)-1-Hydroxy-propyl)-3,5-dimethyl-tetrahydro-furan-2-yl]-butyryl}-4-methyl-5-phenyl-oxazolidin-2-one

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; 3 A molecular sieve; In 2,2,4-trimethylpentane; benzene; for 11h; Ambient temperature;
DOI:10.1021/ja00020a025

Reference yield:

: 135501-76-7
<3(2R,2(2S,3S,5S,5(1R))),4R,5R>-3-<2-(5-(1-hydroxypropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

: 135396-85-9
<3(2R,2(2S,3S,5S)),4R,5R>-3-<2-(5-(1-oxopropyl)-3,5-dimethyltetrahydro-2-furanyl)-1-oxobutyl>-4-methyl-5-phenyl-2-oxazolidinone

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, -78 deg C, 1 h, 2.) CH₂Cl₂, a) -78 deg C, 1 h, b) 0 deg C, 1.5 h;
DOI:10.1021/ja00020a025