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C38H52O11Si

Base Information
  • Chemical Name:C38H52O11Si
  • CAS No.:1417202-86-8
  • Molecular Formula:C38H52O11Si
  • Molecular Weight:712.91
  • Hs Code.:
C<sub>38</sub>H<sub>52</sub>O<sub>11</sub>Si

Synonyms:C38H52O11Si

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Chemical Property of C38H52O11Si
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Technology Process of C38H52O11Si

There total 4 articles about C38H52O11Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine; triphenylphosphine; In toluene; at 70 ℃; for 18h;
DOI:10.1002/chem.201201624
Guidance literature:
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; triethylamine / toluene
2: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; diisopropylamine / toluene / 20 h / 80 °C / Inert atmosphere
3: iodine; methyl iodide / 22 h / 115 °C
4: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; triethylamine / toluene / 18 h / 70 °C
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); iodine; triethylamine; diisopropylamine; triphenylphosphine; methyl iodide; In toluene; 1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201201624
Guidance literature:
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; diisopropylamine / toluene / 20 h / 80 °C / Inert atmosphere
2: iodine; methyl iodide / 22 h / 115 °C
3: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; triethylamine / toluene / 18 h / 70 °C
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); iodine; triethylamine; diisopropylamine; triphenylphosphine; methyl iodide; In toluene; 1: |Sonogashira Cross-Coupling / 3: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201201624
upstream raw materials:

C37H53N3O11

C33H43IO11

trimethylsilylacetylene

C18H28BrN3O5

Downstream raw materials:

C35H44O11

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