(Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

Base Information

Chemical Name:(Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle
CAS No.:119099-63-7
Molecular Formula:C₁₅H₁₉NO₄S
Molecular Weight:309.386
Hs Code.:

Synonyms:(Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

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Technology Process of (Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

There total 1 articles about (Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2958-89-6
N-(chlorosulfanyl)morpholine

: 18020-59-2
methyl 3-hydroxy-2-methylidene-3-phenylpropionate

: 119099-63-7
(Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

Guidance literature:: With triethylamine; In diethyl ether; at -78 - 20 ℃;
DOI:10.1016/0040-4039(88)85134-7

Reference yield: 92.0%

: 119099-63-7
(Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

: 119099-79-5
(Z)-3-phenyl-2-(sulfinomethyl)prop-2-enoate de methyle

Guidance literature:: With methanesulfonic acid; water; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/0040-4039(88)85135-9

Reference yield:

: 119099-63-7
(Z)-4-<(morpholin-4-ylsulfinyl)methyl>-3-phenylprop-2-enoate de methyle

: 2-<(methylsulfonyl)methyl>-3-phenylprop-2-enoate de methyle

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 3 equiv water, 1 equiv methanesulfonic acid / tetrahydrofuran / 2 h / 0 °C

2: 74 percent / potassium carbonate / tetrahydrofuran; dimethylformamide

With methanesulfonic acid; water; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(88)85135-9