3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane

Base Information

• Chemical Name: 3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane
• CAS No.: 249641-01-8
• Molecular Formula: C₁₂H₁₉NO₂S₂Si
• Molecular Weight: 301.506
• Mol file: 249641-01-8.mol

Synonyms:3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane

Chemical Property of 3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane

There total 1 articles about 3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

chloramine-B (127-52-6) + 3,3-dimethyl-1-thia-3-silacyclopentane (18163-14-9) → 3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane (249641-01-8)

Guidance literature:

With tetraethylbenzylammonium chloride; In dichloromethane;

DOI:10.1016/S0022-328X(03)00348-6

Reference yield: 80.0%

3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane (249641-01-8) → C12H21NO3S2Si (600156-73-8)

Guidance literature:

With potassium hydroxide; water; at 20 ℃; for 0.25h;

DOI:10.1016/S0022-328X(03)00348-6

Reference yield:

3-(benzenesulfonylimino)-1,1-dimethyl-1,3-silathiane (249641-01-8) → C24H40N2O5S4Si2

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / KOH; waater / 0.25 h / 20 °C

2: NaHCO₃; water

With potassium hydroxide; water; sodium hydrogencarbonate;

DOI:10.1016/S0022-328X(03)00348-6

upstream raw materials:

chloramine-B

3,3-dimethyl-1-thia-3-silacyclopentane

Downstream raw materials:

C₁₂H₂₁NO₃S₂Si