3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

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Chemical Name:3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole
CAS No.:76451-83-7
Molecular Formula:C₁₄H₁₄Cl₂N₂O
Molecular Weight:297.184
Hs Code.:

Synonyms:3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

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Technology Process of 3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

There total 4 articles about 3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76439-22-0
1-[(4S,5S)-3-(2,6-Dichloro-phenyl)-5-pyrrolidin-1-yl-4,5-dihydro-isoxazol-4-ylmethyl]-1-methyl-pyrrolidinium; iodide

: 76451-83-7
3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

Guidance literature:: With triethylamine; at 40 ℃;

Reference yield:

: 76439-25-3
C₁₁H₂₀N₂

: 76451-83-7
3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / Ambient temperature

2: 70 percent / acetonitrile / Ambient temperature

3: 70 percent / triethylamine / 40 °C

With triethylamine; In acetonitrile;

Reference yield:

: 76439-15-1
(4S,5S)-3-(2,6-Dichloro-phenyl)-5-pyrrolidin-1-yl-4-pyrrolidin-1-ylmethyl-4,5-dihydro-isoxazole

: 76451-83-7
3-(2,6-Dichloro-phenyl)-4-methylene-5-pyrrolidin-1-yl-4,5-dihydro-isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetonitrile / Ambient temperature

2: 70 percent / triethylamine / 40 °C

With triethylamine; In acetonitrile;