1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

Base Information

Chemical Name:1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit
CAS No.:90626-66-7
Molecular Formula:C₂₄H₃₆O₈
Molecular Weight:452.545
Hs Code.:

Synonyms:1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

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Chemical Property of 1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

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Technology Process of 1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

There total 6 articles about 1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 90626-65-6
1L-4-O-Benzyl-3-desoxy-3-C-hydroxymethyl-1,2:5,6-di-O-isopropyliden-allo-inosit

: 90626-66-7
1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;

Reference yield:

: 65533-41-7
1L-4-O-Benzyl-1,2:5,6-di-O-isopropyliden-chiro-inosit

: 90626-66-7
1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

Guidance literature:: Multi-step reaction with 4 steps

1: 1) DMSO, oxalylchloride; 2) ethyl diisopropylamine / 1) CH₂Cl₂, -78 deg C, 310 min; CH₂Cl₂, 30 min; 2) room temp., 30 min

2: 1) n-LiBu / 1) -30 deg C, hexane, THF, 30 min; 2) THF, room temp., 2 h

3: 1) BH₃*THF, methyl-2-buten / 1) THF, 0 deg C; 2) THF, room temp.; 3 h, reflux

4: 85 percent / diisopropylethylamine / CH₂Cl₂

With n-butyllithium; borane-THF; Chloro-oxo-acetic acid; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-pentene; In dichloromethane;

Reference yield:

: 90626-63-4
2D-(2,3,6/4,5)-6-O-Benzyl-2,3:4,5-di-O-isopropyliden-1-methylen-2,3,4,5,6-cyclohexan-pentol

: 90626-66-7
1L-4-O-Benzyl-3-desoxy-1,2:5,6-di-O-isopropyliden-3-C-<(2-methoxyethoxy)methoxymethyl>-allo-inosit

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BH₃*THF, methyl-2-buten / 1) THF, 0 deg C; 2) THF, room temp.; 3 h, reflux

2: 85 percent / diisopropylethylamine / CH₂Cl₂

With borane-THF; N-ethyl-N,N-diisopropylamine; 2-pentene; In dichloromethane;