1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

Base Information

Chemical Name:1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione
CAS No.:1354708-17-0
Molecular Formula:C₂₉H₄₀O₇
Molecular Weight:500.632
Hs Code.:

Synonyms:1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

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Chemical Property of 1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

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Technology Process of 1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

There total 2 articles about 1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1354708-12-5
4'-decyl-2-methoxy-2'-(2'',4'',6''-trimethoxybenzoyloxy)acetophenone

: 1354708-17-0
1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

Guidance literature:: 4'-decyl-2-methoxy-2'-(2'',4'',6''-trimethoxybenzoyloxy)acetophenone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -20 ℃; for 1h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at -20 ℃; Inert atmosphere;
DOI:10.1139/v11-087

Reference yield:

: 649551-92-8
2'-hydroxy-4'-decyl-2-methoxy-acetophenone

: 1354708-17-0
1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere

2.2: -20 °C / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; 2.1: Baker-Venkataraman rearrangement;
DOI:10.1139/v11-087

Reference yield: 37.0%

: 1354708-17-0
1-(4'-decyl-2'-hydroxyphenyl)-2-methoxy-3-(2'',4'',6''-trimethoxyphenyl)propane-1,3-dione

: 1354708-25-0
7-decyl-3,2',4',6'-tetramethoxyflavone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1139/v11-087