2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Base Information

Chemical Name:2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane
CAS No.:74431-09-7
Molecular Formula:C₁₃H₁₅N₂O₈P
Molecular Weight:358.244
Hs Code.:

Synonyms:2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

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Chemical Property of 2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

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Technology Process of 2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

There total 10 articles about 2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 20056-44-4
2,4-dinitrophenyl phosphorodichloridate

: 27583-43-3
2-(hydroxymethyl)cyclohexanol

: 74431-09-7
2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

: 74378-78-2,74410-70-1,74431-09-7
2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Guidance literature:: With pyridine; In chloroform; at 0 ℃; for 6h;
DOI:10.1002/hlca.19970800208

Reference yield: 11.0%

: 20056-44-4
2,4-dinitrophenyl phosphorodichloridate

: 27583-43-3
2-(hydroxymethyl)cyclohexanol

: 74431-09-7
2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

: 74378-78-2,74410-70-1,74431-09-7
2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Guidance literature:: With pyridine; In chloroform; at 0 ℃; for 6h;
DOI:10.1002/hlca.19970800208

Reference yield:

: 4187-59-1,4187-60-4,27583-43-3,29569-80-0,51606-49-6,51606-50-9,69308-85-6,96553-66-1,106758-67-2
trans-2-hydroxymethylcyclohexanol

: 74431-09-7
2-(2,4-dinitrophenoxy)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃ / diethyl ether / 1 h / 0 °C

2: toluene / 90 °C

With trichlorophosphate; In diethyl ether; toluene;
DOI:10.1021/ja00535a044