(E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

Base Information

Chemical Name:(E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester
CAS No.:157055-06-6
Molecular Formula:C₂₀H₂₉NO₅
Molecular Weight:363.454
Hs Code.:

Synonyms:(E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

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Chemical Property of (E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

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Technology Process of (E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

There total 1 articles about (E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 124957-48-8
(E)-2-(Isopropylamino-methyl)-3-(2-methoxy-phenyl)-acrylic acid methyl ester

: 157055-06-6
(E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

Guidance literature:: With sodium hydroxide; In dichloromethane; at 10 ℃; for 12h;
DOI:10.1080/00397919408011492

Reference yield:

: 157055-06-6
(E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

: 157055-12-4
3-(tert-Butoxycarbonyl-isopropyl-amino)-2-(2-methoxy-benzyl)-propionic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 0.333333h; under 760 Torr;
DOI:10.1080/00397919408011492

Reference yield:

: 157055-06-6
(E)-2-[(tert-Butoxycarbonyl-isopropyl-amino)-methyl]-3-(2-methoxy-phenyl)-acrylic acid methyl ester

: 2-(Isopropylamino-methyl)-3-(2-methoxy-phenyl)-propionic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 0.33 h / 760 Torr

2: 81 percent / HCl / ethyl acetate / 12 h

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate;
DOI:10.1080/00397919408011492