cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

Base Information

Chemical Name:cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole
CAS No.:98151-47-4
Molecular Formula:C₁₃H₁₄Cl₃NO₃
Molecular Weight:338.618
Hs Code.:

Synonyms:cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

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Chemical Property of cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

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Technology Process of cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

There total 4 articles about cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 98151-46-3
threo-4-benzyloxy-3-iodo-2-trichloroacetamidobutan-1-ol

: 98151-48-5
cis-2-benzyloxymethyl-3-hydroxymethyl-aziridine

: 98151-47-4
cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

Guidance literature:: With Amberlyst A 26; In methanol; at 0 ℃; for 0.5h;

Reference yield:

: 81028-03-7
(Z)-4-benzyloxy-but-2-en-1-ol

: 98151-47-4
cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NaH / tetrahydrofuran / 1.5 h / Ambient temperature

2: 100 percent / N-iodosuccinimide / CHCl₃ / 6 h / Ambient temperature

3: 82 percent / water / methanol / 20 h / Heating

4: 30 percent / Amberlyst A 26 / methanol / 0.5 h / 0 °C

With N-iodo-succinimide; Amberlyst A 26; water; sodium hydride; In tetrahydrofuran; methanol; chloroform;

Reference yield:

: 104808-71-1
erythro-4-<2-(benzyloxy)-1-iodoethyl>-2-(trichloromethyl)-4,5-dihydro-1,3-oxazole

: 98151-47-4
cis-5-benzyloxymethyl-4-hydroxymethyl-2-trichloromethyl-4,5-dihydro-oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / water / methanol / 20 h / Heating

2: 30 percent / Amberlyst A 26 / methanol / 0.5 h / 0 °C

With Amberlyst A 26; water; In methanol;