2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

Base Information

Chemical Name:2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline
CAS No.:1308292-81-0
Molecular Formula:C₂₄H₂₃NO₈
Molecular Weight:453.449
Hs Code.:

Synonyms:2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

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Chemical Property of 2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

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Technology Process of 2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

There total 4 articles about 2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1308292-83-2
C₃₁H₂₉NO₁₀

: 1308292-81-0
2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

Guidance literature:: With iron(III) chloride; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.carres.2011.02.018

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 1308292-81-0
2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 7 h / 60 °C

2.1: pyridine / 72 h / 60 °C

2.2: 48 h / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / 0.5 h / 0 - 20 °C

4.1: iron(III) chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridine; iron(III) chloride; boron trifluoride diethyl etherate; In pyridine; dichloromethane;
DOI:10.1016/j.carres.2011.02.018

Reference yield:

: C₄₈H₄₁NO₉

: 1308292-81-0
2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / 0.5 h / 0 - 20 °C

2: iron(III) chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

With iron(III) chloride; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/j.carres.2011.02.018