(2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

Base Information

Chemical Name:(2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester
CAS No.:170745-40-1
Molecular Formula:C₂₀H₂₇NO₆
Molecular Weight:377.437
Hs Code.:

Synonyms:(2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

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Chemical Property of (2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

Chemical Property:

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Technology Process of (2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

There total 2 articles about (2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24850-33-7
allyltributylstanane

: (S)-2-Benzyloxycarbonylamino-3-phenylselanyl-succinic acid 1-tert-butyl ester 4-methyl ester

: 170745-40-1
(2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

: (2R,3R)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In toluene; at -40 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;
DOI:10.1021/ja953913f

Reference yield:

: 106-95-6
allyl bromide

: 149967-06-6
N-<(phenylmethoxy)carbonyl>-D-aspartic acid, 1-(1,1-dimethylethyl) 4-methyl ester

: 170745-40-1
(2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

: (2R,3R)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 25 ℃; for 1h;
DOI:10.1016/0040-4020(95)00454-G

Reference yield:

: 170745-40-1
(2R,3S)-2-Allyl-3-benzyloxycarbonylamino-succinic acid 4-tert-butyl ester 1-methyl ester

: (2R,3S)-5-Hydroxy-pyrrolidine-1,2,3-tricarboxylic acid 1-benzyl ester 2-tert-butyl ester 3-methyl ester

: (2R,3S)-5-Methoxy-pyrrolidine-1,2,3-tricarboxylic acid 1-benzyl ester 2-tert-butyl ester 3-methyl ester

Guidance literature:: With dimethylsulfide; ozone; acetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂/MeOH, -78 deg C; 2.) CH₂Cl₂/MeOH, r.t., 72 h;
DOI:10.1016/0040-4020(95)00454-G