C₃₁H₅₂O₆Si

Base Information

Chemical Name:C₃₁H₅₂O₆Si
CAS No.:934617-92-2
Molecular Formula:C₃₁H₅₂O₆Si
Molecular Weight:548.836
Hs Code.:

C<sub>31</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C₃₁H₅₂O₆Si

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Chemical Property of C₃₁H₅₂O₆Si

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Technology Process of C₃₁H₅₂O₆Si

There total 25 articles about C₃₁H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 934617-91-1
C₃₁H₅₁BrO₆Si

: 934617-92-2
C₃₁H₅₂O₆Si

Guidance literature:: With triethyl borane; tri-n-butyl-tin hydride; In toluene; at 0 ℃;
DOI:10.1246/cl.2007.278

Reference yield:

: 934617-86-4
C₃₇H₆₈O₆SSi₂

: 934617-92-2
C₃₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: 100 percent / TEA; DMAP / CH₂Cl₂

2.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

3.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

4.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

5.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

6.1: 65 percent / Eu(fod)3 / xylene / 120 °C

7.1: 99 percent / AgNO₃; pyridine / acetonitrile

8.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

9.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

9.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

10.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

11.1: 97 percent / DMAP; TEA / CH₂Cl₂

12.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / 50 °C

12.2: 38 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

13.1: 59 percent / n-BuLi; DIBAL / toluene

14.1: 98 percent / TEA; DMAP / CH₂Cl₂

15.1: 93 percent / AcOH; H₂O / tetrahydrofuran

16.1: pyridine / CH₂Cl₂

17.1: n-Bu₄NBr / toluene / 50 °C

18.1: 74 percent / Bu₃SnH; Et₃B / toluene / 0 °C

With pyridine; quinoline; dmap; sodium tetrahydroborate; n-butyllithium; triethyl borane; TEA; diphenyl diselenide; tetrabutylammomium bromide; water; hydrogen; tri-n-butyl-tin hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278

Reference yield:

: 934617-99-9
C₃₂H₅₆O₈S₂Si

: 934617-92-2
C₃₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

2.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

3.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

4.1: 65 percent / Eu(fod)3 / xylene / 120 °C

5.1: 99 percent / AgNO₃; pyridine / acetonitrile

6.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

7.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

7.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

8.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

9.1: 97 percent / DMAP; TEA / CH₂Cl₂

10.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / 50 °C

10.2: 38 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

11.1: 59 percent / n-BuLi; DIBAL / toluene

12.1: 98 percent / TEA; DMAP / CH₂Cl₂

13.1: 93 percent / AcOH; H₂O / tetrahydrofuran

14.1: pyridine / CH₂Cl₂

15.1: n-Bu₄NBr / toluene / 50 °C

16.1: 74 percent / Bu₃SnH; Et₃B / toluene / 0 °C

With pyridine; quinoline; dmap; sodium tetrahydroborate; n-butyllithium; triethyl borane; TEA; diphenyl diselenide; tetrabutylammomium bromide; water; hydrogen; tri-n-butyl-tin hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278