2-nitro-3,4,6-trichlorobenzaldehyde

Base Information

• Chemical Name: 2-nitro-3,4,6-trichlorobenzaldehyde
• CAS No.: 1086838-05-2
• Molecular Formula: C₇H₂Cl₃NO₃
• Molecular Weight: 254.457
• Mol file: 1086838-05-2.mol

Synonyms:2-nitro-3,4,6-trichlorobenzaldehyde

Chemical Property of 2-nitro-3,4,6-trichlorobenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-nitro-3,4,6-trichlorobenzaldehyde

There total 6 articles about 2-nitro-3,4,6-trichlorobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C8H4Cl3NO5 → 2-nitro-3,4,6-trichlorobenzaldehyde (1086838-05-2)

Guidance literature:

With dimethylsulfide; In methanol; dichloromethane; at -78 ℃;

Reference yield:

2-nitro-3,4,6-trichloroaniline (40157-48-0) → 2-nitro-3,4,6-trichlorobenzaldehyde (1086838-05-2)

Guidance literature:

Multi-step reaction with 3 steps

1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 60 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dichloromethane; toluene / 24 h / 100 °C

3: ozone / dichloromethane; methanol / 2 h / -78 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert.-butylnitrite; ozone; copper(ll) bromide; In methanol; dichloromethane; toluene; acetonitrile;

Reference yield:

2,4,5-trichloroaniline (636-30-6) → 2-nitro-3,4,6-trichlorobenzaldehyde (1086838-05-2)

Guidance literature:

Multi-step reaction with 6 steps

1: 20 - 25 °C

2: nitric acid; sulfuric acid / 5 h / 0 - 25 °C

3: hydrogenchloride / 1,4-dioxane / Reflux

4: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 60 °C

5: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dichloromethane; toluene / 24 h / 100 °C

6: ozone / dichloromethane; methanol / 2 h / -78 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert.-butylnitrite; sulfuric acid; nitric acid; ozone; copper(ll) bromide; In 1,4-dioxane; methanol; dichloromethane; toluene; acetonitrile;

upstream raw materials:

2-nitro-3,4,6-trichloroaniline

2,4,5-trichloroaniline

N-(2,4,5-trichlorophenyl)acetamide

N-(2-nitro-3,4,6-trichlorophenyl)-acetamide