dicamba 6-nitroveratryl alcohol ester

Base Information

• Chemical Name: dicamba 6-nitroveratryl alcohol ester
• CAS No.: 1430102-78-5
• Molecular Formula: C₁₇H₁₅Cl₂NO₇
• Molecular Weight: 416.215
• Mol file: 1430102-78-5.mol

Synonyms:dicamba 6-nitroveratryl alcohol ester

Chemical Property of dicamba 6-nitroveratryl alcohol ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dicamba 6-nitroveratryl alcohol ester

There total 10 articles about dicamba 6-nitroveratryl alcohol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

6-nitroveratryl alcohol (1016-58-6) + 3,6-dichloro-2-methoxybenzoic acid chloride (10411-85-5) → dicamba 6-nitroveratryl alcohol ester (1430102-78-5)

Guidance literature:

With dmap; triethylamine; In chloroform; for 70h; Darkness;

Reference yield:

dicamba 4-butoxyphenacylmethyl ester (1430102-83-2) → dicamba 6-nitroveratryl alcohol ester (1430102-78-5)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 168 h / 35 °C / Sealed tube; UV-irradiation

2: thionyl chloride / 2.5 h / 80 °C

3: triethylamine; dmap / chloroform / 70 h / Darkness

With dmap; thionyl chloride; triethylamine; In tetrahydrofuran; chloroform;

Reference yield:

dicamba 4-methoxyphenacylmethyl ester (1430102-82-1) → dicamba 6-nitroveratryl alcohol ester (1430102-78-5)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 28 h / 35 °C / Sealed tube; UV-irradiation

2: thionyl chloride / 2.5 h / 80 °C

3: triethylamine; dmap / chloroform / 70 h / Darkness

With dmap; thionyl chloride; triethylamine; In tetrahydrofuran; chloroform;

upstream raw materials:

6-nitroveratryl alcohol

3,6-dichloro-2-methoxybenzoic acid chloride

dicamba 4-methoxyphenacylmethyl ester

dicamba 4-butoxyphenacylmethyl ester