3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

Base Information

Chemical Name:3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester
CAS No.:233692-14-3
Molecular Formula:C₂₇H₃₄N₂O₇
Molecular Weight:498.576
Hs Code.:

3-(2-<i>tert</i>-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

Synonyms:3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

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Chemical Property of 3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

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Technology Process of 3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

There total 3 articles about 3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 233692-13-2
BOC-(L)-Glu(OiPr)-OH

: 3-aminobenzoic acid benzyl ester toluene-4-sulfonate

: 233692-14-3
3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; chlorotri(pyrrolidin-1-yl)phosphonium hexafluorophosphate; In dichloromethane; Ambient temperature;
DOI:10.1021/ja983970j

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 233692-14-3
3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / dioxane; H₂O / 4 h / Ambient temperature

2: 87 percent / chlorotripyrrolidinophosphonium hexafluorophosphate, N-ethyldiisopropylamine / CH₂Cl₂ / Ambient temperature

With triethylamine; N-ethyl-N,N-diisopropylamine; chlorotri(pyrrolidin-1-yl)phosphonium hexafluorophosphate; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/ja983970j

Reference yield:

: 16652-44-1
L-glutamic acid 5-isopropyl ester

: 233692-14-3
3-(2-tert-butoxycarbonylamino-4-isopropoxycarbonyl-butyrylamino)-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / dioxane; H₂O / 4 h / Ambient temperature

2: 87 percent / chlorotripyrrolidinophosphonium hexafluorophosphate, N-ethyldiisopropylamine / CH₂Cl₂ / Ambient temperature

With triethylamine; N-ethyl-N,N-diisopropylamine; chlorotri(pyrrolidin-1-yl)phosphonium hexafluorophosphate; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/ja983970j