4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol

Base Information

• Chemical Name: 4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol
• CAS No.: 1198401-43-2
• Molecular Formula: C₂₆H₂₂O₃
• Molecular Weight: 382.459

Synonyms:4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol

Chemical Property of 4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol

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Technology Process of 4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol

There total 2 articles about 4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C26H23BrO3 → 4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol (1198401-43-2)

Guidance literature:

With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tBu₄NOAc; lithium acetate; In water; N,N-dimethyl-formamide; acetonitrile; at 120 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja906260x

Reference yield: 58.0%

C26H23BrO3 → 4-[2-(cyclohex-2-enyloxy)phenyl]-2,3-dihydro-1-oxa-cyclopenta[def]phenanthren-3-ol (1198401-43-2) + C20H14O3

Guidance literature:

With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); lithium acetate; tetrabutylammonium acetate; In water; N,N-dimethyl-formamide; acetonitrile; at 140 ℃; for 0.75h; Microwave irradiation; Inert atmosphere;

DOI:10.1002/ejoc.201801289

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