2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline

Base Information

• Chemical Name: 2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline
• CAS No.: 1053223-34-9
• Molecular Formula: C₂₄H₂₃NO₆
• Molecular Weight: 421.45

Synonyms:2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline

Chemical Property of 2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline

Chemical Property:

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Technology Process of 2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline

There total 1 articles about 2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

cinnamoyl chloride (102-92-1,17082-09-6) + 2-methyl-4,5-(3-O-acetyl-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline (257927-02-9) → 2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline (1053223-34-9)

Guidance literature:

2-methyl-4,5-(3-O-acetyl-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline; With sodium methylate; In methanol; at 20 ℃; for 1h;

In methanol; for 0.333333h;

cinnamoyl chloride; With pyridine; In dichloromethane; at 20 ℃;

DOI:10.1021/jo801037z

Reference yield: 100.0%

2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline (1053223-34-9) → C24H25NO6 (1053223-36-1)

Guidance literature:

With 10% Pd on charcoal; hydrogen; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1021/jo801037z

Reference yield: 74.0%

2-methyl-4,5-(3-O-(trans-3-phenylacryloyl)-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline (1053223-34-9) → 2-acetamido-1,5-anhydro-4,6-O-benzylidene-3-O-(3-phenylpropionyl)-2-deoxy-D-glucitol (1053223-35-0)

Guidance literature:

With 10% Pd on charcoal; hydrogen; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1021/jo801037z

upstream raw materials:

cinnamoyl chloride

2-methyl-4,5-(3-O-acetyl-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline

Downstream raw materials:

C₂₄H₂₅NO₆

2-acetamido-1,5-anhydro-4,6-O-benzylidene-3-O-(3-phenylpropionyl)-2-deoxy-D-glucitol

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