(R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

Base Information

Chemical Name:(R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid
CAS No.:224964-50-5
Molecular Formula:C₂₁H₂₇NO₈
Molecular Weight:421.447
Hs Code.:

Synonyms:(R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

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Chemical Property of (R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

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Technology Process of (R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

There total 2 articles about (R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7474-05-7
(R)-2-chloropropionic acid

: 74984-84-2
prop-2-en-1-yl 2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 224964-50-5
(R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 70 ℃; for 18h;

Reference yield:

: 1171121-75-7
C₁₉H₂₅NO₇

: 108-24-7
acetic anhydride

: 224964-50-5
(R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1080/07328303.2010.512405

Reference yield: 90.0%

: 224964-50-5
(R)-2-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

: (R)-4-{(S)-5-Acetylamino-1-[(R)-1-((R)-1-benzyloxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-pentylcarbamoyl}-2-((R)-2-amino-propionylamino)-butyric acid benzyl ester

: 224964-56-1
2-{2-[2-(7-acetylamino-6-allyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-4-{5-acetylamino-1-[1-(1-benzyloxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-pentylcarbamoyl}-butyric acid benzyl ester

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 4h; Ambient temperature;