(S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

Base Information

Chemical Name:(S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde
CAS No.:152998-17-9
Molecular Formula:C₂₃H₃₂O₃Si
Molecular Weight:384.591
Hs Code.:

Synonyms:(S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

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Technology Process of (S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

There total 5 articles about (S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: (2R,3S)-5-(tert-Butyl-diphenyl-silanyloxy)-3-methoxy-4,4-dimethyl-pentane-1,2-diol

: 152998-17-9
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 23 ℃;
DOI:10.1016/S0040-4039(00)73924-4

Reference yield:

: 152998-15-7
(S)-3-((R)-2,2-Diethyl-[1,3]dioxolan-4-yl)-3-methoxy-2,2-dimethyl-propan-1-ol

: 152998-17-9
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / imidazole / dimethylformamide / 60 °C

2: HCO₂H / methanol / 23 °C

3: 78 percent / NaIO₄ / tetrahydrofuran; H₂O / 23 °C

With 1H-imidazole; sodium periodate; formic acid; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)73924-4

Reference yield:

: 152998-13-5
(S)-1-((R)-2,2-Diethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-but-3-en-1-ol

: 152998-17-9
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-3,3-dimethyl-butyraldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / NaH / dimethylformamide / 23 °C

2: 1.) O₃; 2.) NaBH₄ / 1.) -78 deg C, CH₂Cl₂-MeOH; 2.) EtOH

3: 86 percent / imidazole / dimethylformamide / 60 °C

4: HCO₂H / methanol / 23 °C

5: 78 percent / NaIO₄ / tetrahydrofuran; H₂O / 23 °C

With 1H-imidazole; sodium tetrahydroborate; sodium periodate; formic acid; sodium hydride; ozone; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)73924-4