C₄₁H₄₉O₈NSi

Base Information

Chemical Name:C₄₁H₄₉O₈NSi
CAS No.:250355-91-0
Molecular Formula:C₄₁H₄₉NO₈Si
Molecular Weight:711.927
Hs Code.:

C<sub>41</sub>H<sub>49</sub>O<sub>8</sub>NSi

Synonyms:C₄₁H₄₉O₈NSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₉O₈NSi

Chemical Property:

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Technology Process of C₄₁H₄₉O₈NSi

There total 9 articles about C₄₁H₄₉O₈NSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-6-vinyl-tetrahydro-pyran-4-one

: 250355-91-0
C₄₁H₄₉O₈NSi

Guidance literature:: Multi-step reaction with 8 steps

1: Rh(PPh₃)3Cl / 23 °C

2: NaBO₃*4H₂O

3: 78 percent / LDA

4: 92 percent / Sn(OTf)2; N-ethylpiperidine

5: 98 percent / LiOH; H₂O₂

6: CH₂Cl₂ / 12 h

7: TMSOTf; triethylamine / CH₂Cl₂ / 65 h / -78 - -25 °C

With 1-ethyl-piperidine; sodium perborate; lithium hydroxide; tin(II) trifluoromethanesulfonate; trimethylsilyl trifluoromethanesulfonate; dihydrogen peroxide; triethylamine; lithium diisopropyl amide; Wilkinson's catalyst; In dichloromethane; 3: Wittig olefination / 4: Swern oxidation;
DOI:10.1021/ol990830l

Reference yield:

: 112897-03-7
3-(tert-butyldiphenylsilyloxy)-1-propanal

: 250355-91-0
C₄₁H₄₉O₈NSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: (R)-BINOL; titanium tetraisopropoxide; trifluoroacetic acid / diethyl ether / 45 h / -78 - -20 °C

1.2: CuI; TMSCl; DMPU

2.1: Rh(PPh₃)3Cl / 23 °C

3.1: NaBO₃*4H₂O

4.1: 78 percent / LDA

5.1: 92 percent / Sn(OTf)2; N-ethylpiperidine

6.1: 98 percent / LiOH; H₂O₂

7.1: CH₂Cl₂ / 12 h

8.1: TMSOTf; triethylamine / CH₂Cl₂ / 65 h / -78 - -25 °C

With 1-ethyl-piperidine; titanium(IV) isopropylate; sodium perborate; lithium hydroxide; tin(II) trifluoromethanesulfonate; trimethylsilyl trifluoromethanesulfonate; dihydrogen peroxide; (R)-1,1'-Bi-2-naphthol; triethylamine; trifluoroacetic acid; lithium diisopropyl amide; Wilkinson's catalyst; In diethyl ether; dichloromethane; 1.1: Diels-Alder reaction / 4.1: Wittig olefination / 5.1: Swern oxidation;
DOI:10.1021/ol990830l

Reference yield:

: C₃₄H₅₄O₅Si₃

: 224578-16-9
2-(4-Methoxy-benzyloxymethyl)-oxazole-4-carbaldehyde

: 250355-91-0
C₄₁H₄₉O₈NSi

: C₄₁H₄₉O₈NSi

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at -78 - -25 ℃; for 65h;
DOI:10.1021/ol990830l