N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

Base Information

Chemical Name:N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine
CAS No.:1421133-01-8
Molecular Formula:C₁₁H₄BrF₁₂NO₃S₂
Molecular Weight:570.174
Hs Code.:

Synonyms:N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

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Chemical Property of N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

Chemical Property:

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Technology Process of N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

There total 3 articles about N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1178899-43-8
(4-bromophenyl)(imino)(perfluorobutyl)-λ⁶-sulfanone

: 1421133-01-8
N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

Guidance literature:: (4-bromophenyl)(imino)(perfluorobutyl)-λ⁶-sulfanone; With sodium hydride; In dichloromethane; mineral oil; at 0 ℃; for 1h; Inert atmosphere; Reflux;

trifluoromethylsulfonic anhydride; In dichloromethane; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/chem.201103460

Reference yield:

: 1178899-47-2
nonafluorobutyl p-bromophenyl sulfoxide

: 1421133-01-8
N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; trifluoromethylsulfonic anhydride / 16 h / -15 °C / Inert atmosphere

2.1: sodium hydroxide; potassium permanganate / water / 2 h / Inert atmosphere

3.1: sodium hydride / mineral oil; dichloromethane / 1 h / 0 °C / Inert atmosphere; Reflux

3.2: 16 h / Reflux; Inert atmosphere

With potassium permanganate; trifluoromethylsulfonic anhydride; sodium hydride; sodium hydroxide; In dichloromethane; water; mineral oil;
DOI:10.1002/chem.201103460

Reference yield:

: 1178899-27-8
N-acetyl-S-(p-bromophenyl)-S-(nonafluorobutyl)sulfilimine

: 1421133-01-8
N-trifluoromethylsulfonyl-S-nonafluorobutyl-S-p-bromophenylsulfoximine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; potassium permanganate / water / 2 h / Inert atmosphere

2.1: sodium hydride / mineral oil; dichloromethane / 1 h / 0 °C / Inert atmosphere; Reflux

2.2: 16 h / Reflux; Inert atmosphere

With potassium permanganate; sodium hydride; sodium hydroxide; In dichloromethane; water; mineral oil;
DOI:10.1002/chem.201103460