Technology Process of C56H57N13O11S6
There total 8 articles about C56H57N13O11S6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methyl adipoyl chloride; C2HF3O2*C49H47N13O8S6;
With
pyridine;
at 20 ℃;
for 0.166667h;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
2.1: chloroformic acid ethyl ester; triethylamine / acetone / 1 h
2.2: 1.33 h / 60 °C
3.1: 2 h / 80 °C
4.1: pyridine; dmap / 3 h
5.1: dichloromethane / 0.5 h
6.1: water; sodium hydrogencarbonate / ethyl acetate
7.1: pyridine / 0.17 h / 20 °C
With
pyridine; dmap; water; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; ethyl acetate; acetone;
DOI:10.1021/jm200938f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane / 0.5 h
2: water; sodium hydrogencarbonate / ethyl acetate
3: pyridine / 0.17 h / 20 °C
With
pyridine; water; sodium hydrogencarbonate;
In
dichloromethane; ethyl acetate;
DOI:10.1021/jm200938f