Technology Process of C49H48N2O15
There total 10 articles about C49H48N2O15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen fluoride;
In
acetonitrile;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 96 percent / HBr / acetic acid
2: 74 percent / Hg(CN)2
3: 53 percent / aq. HCl / acetone
4: 82 percent / TsOH
5: 91 percent / pyridine
6: 80 percent / NaBH3CN, HCl
7: 77 percent / imidazole
8: 2.) OsO4, Me3NO / 1.) CODIr(PMePh2)2(1+)PF6(1-)
9: 73 percent / pyridine
10: 65 percent / TMSOTf
11: 76 percent / 40percent aq. HF / acetonitrile
With
pyridine; 1H-imidazole; hydrogenchloride; osmium(VIII) oxide; trimethylamine-N-oxide; trimethylsilyl trifluoromethanesulfonate; hydrogen fluoride; hydrogen bromide; mercury(II) cyanide; sodium cyanoborohydride; toluene-4-sulfonic acid;
(bis(diphenylphosphino)ethylene)(1,5-cyclooctadiene)iridium(I) hexafluorophosphate;
In
acetic acid; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 82 percent / TsOH
2: 91 percent / pyridine
3: 80 percent / NaBH3CN, HCl
4: 77 percent / imidazole
5: 2.) OsO4, Me3NO / 1.) CODIr(PMePh2)2(1+)PF6(1-)
6: 73 percent / pyridine
7: 65 percent / TMSOTf
8: 76 percent / 40percent aq. HF / acetonitrile
With
pyridine; 1H-imidazole; hydrogenchloride; osmium(VIII) oxide; trimethylamine-N-oxide; trimethylsilyl trifluoromethanesulfonate; hydrogen fluoride; sodium cyanoborohydride; toluene-4-sulfonic acid;
(bis(diphenylphosphino)ethylene)(1,5-cyclooctadiene)iridium(I) hexafluorophosphate;
In
acetonitrile;
