antimycin A₁₈

Base Information

Chemical Name:antimycin A₁₈
CAS No.:1056986-75-4
Molecular Formula:C₂₃H₃₀N₂O₉
Molecular Weight:478.499
Hs Code.:

Synonyms:antimycin A₁₈

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Chemical Property of antimycin A₁₈

Chemical Property:

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Technology Process of antimycin A₁₈

There total 14 articles about antimycin A₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₃₆N₂O₉

: 1056986-75-4
antimycin A₁₈

Guidance literature:: With palladium on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 2h; under 760.051 Torr;
DOI:10.1002/ejoc.201100034

Reference yield:

: 931581-19-0
C₂₀H₃₀O₅

: 1056986-75-4
antimycin A₁₈

Guidance literature:: Multi-step reaction with 12 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

3: dmap; triethylamine / toluene / 16 h / 0 - 20 °C

4: hydrogenchloride; water / ethanol / 24 h / 20 °C

5: pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine / acetonitrile / 7 h / 0 - 20 °C

6: triphenylphosphine / toluene / 3 h / 20 °C

7: copper(I) trifluoromethanesulfonate benzene / benzene / 3 h / 80 °C

8: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

10: palladium on carbon; hydrogen / tetrahydrofuran / 2 h / 20 °C / 760.05 Torr / Darkness

11: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

12: palladium on carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With pyrrolidine; 4-methyl-morpholine; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) trifluoromethanesulfonate benzene; palladium on carbon; water; hydrogen; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1002/ejoc.201100034

Reference yield:

: 931581-20-3
C₂₉H₅₀O₅Si

: 1056986-75-4
antimycin A₁₈

Guidance literature:: Multi-step reaction with 11 steps

1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

2: dmap; triethylamine / toluene / 16 h / 0 - 20 °C

3: hydrogenchloride; water / ethanol / 24 h / 20 °C

4: pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine / acetonitrile / 7 h / 0 - 20 °C

5: triphenylphosphine / toluene / 3 h / 20 °C

6: copper(I) trifluoromethanesulfonate benzene / benzene / 3 h / 80 °C

7: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

9: palladium on carbon; hydrogen / tetrahydrofuran / 2 h / 20 °C / 760.05 Torr / Darkness

10: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

11: palladium on carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With pyrrolidine; 4-methyl-morpholine; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) trifluoromethanesulfonate benzene; palladium on carbon; water; hydrogen; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1002/ejoc.201100034