12-Dehydrodigoxigenin

Base Information

Chemical Name:12-Dehydrodigoxigenin
CAS No.:2842-85-5
Molecular Formula:C₂₃H₃₂O₅
Molecular Weight:388.504
Hs Code.:
Nikkaji Number:J72.650H
Wikidata:Q76423510
Mol file:2842-85-5.mol

Synonyms:12-Dehydrodigoxigenin;2842-85-5;BRN 1300407;3-beta,14-Dihydroxy-12-oxo-5-beta-card-20(22)-enolide;5-beta-CARD-20(22)-ENOLIDE, 3-beta,14-DIHYDROXY-12-OXO-

Suppliers and Price of 12-Dehydrodigoxigenin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 12-Dehydrodigoxigenin

Chemical Property:

Vapor Pressure:2.1E-16mmHg at 25°C
Boiling Point:590.5°Cat760mmHg
Flash Point:204.3°C
PSA：83.83000
Density:1.292g/cm³
LogP:2.78330
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:388.22497412
Heavy Atom Count:28
Complexity:758

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC12CCC(CC1CCC3C2CC(=O)C4(C3(CCC4C5=CC(=O)OC5)O)C)O
Isomeric SMILES:C[C@]12CC[C@@H](C[C@H]1CC[C@@H]3[C@@H]2CC(=O)[C@]4([C@@]3(CC[C@@H]4C5=CC(=O)OC5)O)C)O

Technology Process of 12-Dehydrodigoxigenin

There total 3 articles about 12-Dehydrodigoxigenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 20830-75-5
digoxin

: 2842-85-5
3β,14-Dihydroxy-12-oxo-5β,14β-card-20(22)-enolid

Guidance literature:: With chromium(VI) oxide; In N,N-dimethyl-formamide; for 30h;
DOI:10.1016/S0040-4039(00)98730-6

Reference yield:

: 2842-85-5
3β,14-Dihydroxy-12-oxo-5β,14β-card-20(22)-enolid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; Yield given. Multistep reaction; 1.) DMF, 40 h, r.t.; 2.) CH₃OH, 35 min., refl.;