Technology Process of C25H24
There total 3 articles about C25H24 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
titanium(IV) dichlorodiisopropylate; sodium hexamethyldisilazane;
In
tetrahydrofuran;
at -20 - 20 ℃;
for 0.75h;
DOI:10.1016/S0040-4020(98)01022-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / triphenylphosphine; copper(I) iodide / palladium acetate / triethylamine / 6 h / Heating
2: 30 percent / TiCl2(OiPr)2; NaN(SiMe3)2 / tetrahydrofuran / 0.75 h / -20 - 20 °C
With
copper(l) iodide; titanium(IV) dichlorodiisopropylate; sodium hexamethyldisilazane; triphenylphosphine;
palladium diacetate;
In
tetrahydrofuran; triethylamine;
1: Arylation / 2: Condensation;
DOI:10.1016/S0040-4020(98)01022-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / triphenylphosphine; copper(I) iodide / palladium acetate / triethylamine / 6 h / Heating
2: 30 percent / TiCl2(OiPr)2; NaN(SiMe3)2 / tetrahydrofuran / 0.75 h / -20 - 20 °C
With
copper(l) iodide; titanium(IV) dichlorodiisopropylate; sodium hexamethyldisilazane; triphenylphosphine;
palladium diacetate;
In
tetrahydrofuran; triethylamine;
1: Arylation / 2: Condensation;
DOI:10.1016/S0040-4020(98)01022-9