1-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane

Base Information

• Chemical Name: 1-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane
• CAS No.: 1396763-87-3
• Molecular Formula: C₈₁H₁₀₄N₄O₁₄Si₂
• Molecular Weight: 1413.91

Synonyms:1-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane

Chemical Property of 1-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane

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Technology Process of 1-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane

There total 1 articles about 1-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.5%

3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-O4-(hydroxyheptyl)thymidine (1396763-85-1) + 3'-O-t-butyldimethylsilyl-5'-O-dimethoxytrityl-1-[5-methyl-4-triazolylpyrimidin-2(1H)-onyl]-β-D-2'-deoxyriboside (80971-34-2) → 1-{O4-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O4-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane (1396763-87-3)

Guidance literature:

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; for 108h;

DOI:10.1039/c2ob25705j

Reference yield: 82.0%

1-{O4-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O4-[3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane (1396763-87-3) → 1-{O4-[5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O4-[5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane (1396763-89-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.416667h;

DOI:10.1039/c2ob25705j

upstream raw materials:

3'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-O₄-(hydroxyheptyl)thymidine

3'-O-t-butyldimethylsilyl-5'-O-dimethoxytrityl-1-[5-methyl-4-triazolylpyrimidin-2(1H)-onyl]-β-D-2'-deoxyriboside

Downstream raw materials:

1-{O₄-[5'-O-(4,4'-dimethoxytrityl)thymidyl]}-7-{O₄-[5'-O-(4,4'-dimethoxytrityl)thymidyl]}heptane

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