C₁₁H₁₃IOS

Base Information

Chemical Name:C₁₁H₁₃IOS
CAS No.:939802-93-4
Molecular Formula:C₁₁H₁₃IOS
Molecular Weight:320.194
Hs Code.:

Synonyms:C₁₁H₁₃IOS

Suppliers and Price of C₁₁H₁₃IOS

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₃IOS

Chemical Property:

Purity/Quality:

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Technology Process of C₁₁H₁₃IOS

There total 1 articles about C₁₁H₁₃IOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1072-72-6
Tetrahydrothiopyran-4-one

: 626-00-6
1,3-Diiodobenzene

: 939802-93-4
C₁₁H₁₃IOS

Guidance literature:: 1,3-Diiodobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

Tetrahydrothiopyran-4-one; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/j.bmcl.2012.09.099

Reference yield:

: 939802-93-4
C₁₁H₁₃IOS

: 939803-04-0
C₂₆H₃₀F₃IN₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; acetic acid / 20 °C

2.1: thiourea / ethanol; acetic acid / Reflux

3.1: p-toluenesulfonyl chloride; 1-methyl-1H-imidazole / acetonitrile / 0 - 20 °C

3.2: 20 °C

With 1-methyl-1H-imidazole; sulfuric acid; acetic acid; thiourea; p-toluenesulfonyl chloride; In ethanol; acetic acid; acetonitrile; 1.1: |Ritter Amidation;
DOI:10.1016/j.bmcl.2012.09.099

Reference yield:

: 939802-93-4
C₁₁H₁₃IOS

: 939802-98-9
C₂₆H₃₂FIN₂O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; acetic acid / 20 °C

2.1: thiourea / ethanol; acetic acid / Reflux

3.1: p-toluenesulfonyl chloride; 1-methyl-1H-imidazole / acetonitrile / 0 - 20 °C

3.2: 20 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

With 1-methyl-1H-imidazole; sulfuric acid; acetic acid; thiourea; p-toluenesulfonyl chloride; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; acetic acid; acetonitrile; 1.1: |Ritter Amidation;
DOI:10.1016/j.bmcl.2012.09.099