C₁₆H₁₃⁽²⁾H₅OS₃

Base Information

Chemical Name:C₁₆H₁₃⁽²⁾H₅OS₃
CAS No.:112399-06-1
Molecular Formula:C₁₆H₁₈OS₃
Molecular Weight:327.477
Hs Code.:

C<sub>16</sub>H<sub>13</sub><sup>(2)</sup>H<sub>5</sub>OS<sub>3</sub>

Synonyms:C₁₆H₁₃⁽²⁾H₅OS₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₃⁽²⁾H₅OS₃

Chemical Property:

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Technology Process of C₁₆H₁₃⁽²⁾H₅OS₃

There total 8 articles about C₁₆H₁₃⁽²⁾H₅OS₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108428-24-6
2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

: 112399-06-1
C₁₆H₁₃⁽²⁾H₅OS₃

Guidance literature:: With deuteriated sodium hydroxide; In tetrahydrofuran; at 85 ℃; for 10h;
DOI:10.1021/ja00212a042

Reference yield:

: 112399-12-9
2,6-bis(bromomethyl) phenyl phenyl sulphide

: 112399-06-1
C₁₆H₁₃⁽²⁾H₅OS₃

Guidance literature:: Multi-step reaction with 3 steps

1: m-chloroperbenzoic acid

3: NaOD/D₂O / tetrahydrofuran / 10 h / 85 °C

With deuteriated sodium hydroxide; water-d2; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;
DOI:10.1039/c39860001359

Reference yield:

: 118-72-9
2,6-dimethylbenzene-1-thiol

: 112399-06-1
C₁₆H₁₃⁽²⁾H₅OS₃

Guidance literature:: Multi-step reaction with 5 steps

1: 60percent sodium hydride, CuI / hexamethylphosphoric acid triamide / 17 h / 105 °C

2: N-bromosuccinimide / CCl₄ / 46 h / 15 °C / Irradiation

3: 81 percent / tetrabutylammonium bromide / benzene; H₂O / 12 h / 50 °C

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

5: 40percent sodium deuterium oxide / tetrahydrofuran / 10 h / 85 °C

With N-Bromosuccinimide; copper(l) iodide; deuteriated sodium hydroxide; tetrabutylammomium bromide; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; benzene;
DOI:10.1021/ja00212a042