N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

Base Information

Chemical Name:N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2
CAS No.:1391748-71-2
Molecular Formula:C₃₂H₄₁N₃O₂
Molecular Weight:501.681
Hs Code.:

Synonyms:N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

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Technology Process of N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

There total 7 articles about N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1391748-92-7
{5-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]pentyl}-(3-phenylpropyl)carbamic acid tert-butyl ester-d2

: 1391748-71-2
N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/anie.201200822

Reference yield:

: 1391748-89-2
(3-phenylpropyl)-[5-(2,2,2-trifluoroacetylamino)pentyl]carbamic acid tert-butyl ester-d2

: 1391748-71-2
N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

Guidance literature:: Multi-step reaction with 4 steps

1: water; sodium hydroxide / methanol / 15 h / 20 °C

2: methanol / 72 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / methanol / 65 h / 40 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With water; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1002/anie.201200822

Reference yield:

: 1391748-90-5
(5-aminopentyl)-(3-phenylpropyl)carbamic acid tert-butyl ester-d2

: 1391748-71-2
N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 72 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / methanol / 65 h / 40 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1002/anie.201200822