(S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate

Base Information

• Chemical Name: (S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate
• CAS No.: 1260378-07-1
• Molecular Formula: C₃₅H₃₇N₃O₅
• Molecular Weight: 579.696

Synonyms:(S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate

Chemical Property of (S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate

Chemical Property:

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Technology Process of (S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate

There total 1 articles about (S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C17H16O3 (1260378-27-5) + (S)-methyl 7-amino-8-oxo-8-(quinolin-8-ylamino)octanoate trifluoroacetate (1286784-03-9) → (S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate (1260378-07-1)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; benzene; at 22 ℃; for 48h;

DOI:10.1016/j.bmcl.2010.09.096

Reference yield: 16.0%

(S,E)-methyl 7-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-8-oxo-8-(quinolin-8-ylamino)octanoate (1260378-07-1) → (S,E)-N(8)-hydroxy-2-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-N(1)-(quinolin-8-yl)octanediamide (1260377-76-1)

Guidance literature:

With hydroxylamine hydrochloride; potassium tert-butylate; In methanol; at 22 ℃;

DOI:10.1016/j.bmcl.2010.09.096

upstream raw materials:

C₁₇H₁₆O₃

(S)-methyl 7-amino-8-oxo-8-(quinolin-8-ylamino)octanoate trifluoroacetate

Downstream raw materials:

(S,E)-N⁽⁸⁾-hydroxy-2-(3-(4-(4-methylbenzyloxy)phenyl)acrylamido)-N⁽¹⁾-(quinolin-8-yl)octanediamide

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