(S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.1^3,7>docosa-3,5,7(22),17,19,20-hexaene

Base Information

• Chemical Name: (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.1^3,7>docosa-3,5,7(22),17,19,20-hexaene
• CAS No.: 120363-42-0
• Molecular Formula: C₂₇H₂₈N₂O₅
• Molecular Weight: 460.53

Synonyms:(S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.1^3,7>docosa-3,5,7(22),17,19,20-hexaene

Chemical Property of (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.1^3,7>docosa-3,5,7(22),17,19,20-hexaene

Chemical Property:

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Technology Process of (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.1^3,7>docosa-3,5,7(22),17,19,20-hexaene

There total 17 articles about (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.1^3,7>docosa-3,5,7(22),17,19,20-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(S)-2-(3-{4-[5-(2-Amino-ethyl)-2-methoxy-phenoxy]-phenyl}-propionylamino)-3-(4-hydroxy-phenyl)-propionic acid; hydrochloride (120363-38-4) → (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.13,7>docosa-3,5,7(22),17,19,20-hexaene (120363-42-0)

Guidance literature:

With diphenylphosphoranyl azide; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 0 ℃; for 72h;

DOI:10.1021/jo00272a003

Reference yield: 68.0%

3-[4-(5-{2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-ethyl}-2-methoxy-phenoxy)-phenyl]-propionic acid pentafluorophenyl ester; hydrochloride (120363-46-4) → (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.13,7>docosa-3,5,7(22),17,19,20-hexaene (120363-42-0)

Guidance literature:

With 1,4-dioxane; pyridine; at 90 ℃; for 1h;

DOI:10.1021/jo00272a003

Reference yield: 25.0%

3-[4-(5-{2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-ethyl}-2-methoxy-phenoxy)-phenyl]-propionic acid; hydrochloride (120363-45-3) → (S)-4-Methoxy-12-<(4-hydroxyphenyl)methyl>-11,14-dioxo-2-oxa-10,13-diazatricclo<15.2.2.13,7>docosa-3,5,7(22),17,19,20-hexaene (120363-42-0)

Guidance literature:

With diphenylphosphoranyl azide; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 0 ℃; for 72h;

DOI:10.1021/jo00272a003

upstream raw materials:

3-[4-(5-{2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-ethyl}-2-methoxy-phenoxy)-phenyl]-propionic acid; hydrochloride

(S)-2-(3-{4-[5-(2-Amino-ethyl)-2-methoxy-phenoxy]-phenyl}-propionylamino)-3-(4-hydroxy-phenyl)-propionic acid; hydrochloride

3-[4-(5-{2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-ethyl}-2-methoxy-phenoxy)-phenyl]-propionic acid pentafluorophenyl ester; hydrochloride

L-Tyr-OMe

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