4-methyl-N-(nonan-5-ylideneamino)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(nonan-5-ylideneamino)benzenesulfonamide
CAS No.:64884-78-2
Molecular Formula:C16H26 N2 O2 S
Molecular Weight:310.461
Hs Code.:
NSC Number:132027
DSSTox Substance ID:DTXSID60983461

Synonyms:64884-78-2;NSC132027;DTXSID60983461;NSC-132027;4-Methyl-N'-(nonan-5-ylidene)benzene-1-sulfonohydrazide

Suppliers and Price of 4-methyl-N-(nonan-5-ylideneamino)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-methyl-N-(nonan-5-ylideneamino)benzenesulfonamide

Chemical Property:

Boiling Point:430.1°Cat760mmHg
Flash Point:213.9°C
Density:1.07g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:310.17149925
Heavy Atom Count:21
Complexity:395

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC(=NNS(=O)(=O)C1=CC=C(C=C1)C)CCCC

Technology Process of 4-methyl-N-(nonan-5-ylideneamino)benzenesulfonamide

There total 1 articles about 4-methyl-N-(nonan-5-ylideneamino)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 502-56-7
nonanone-5

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 64884-78-2
4-methyl-N'-(nonan-5-ylidene)benzenesulfonohydrazide

Guidance literature:: With hydrogenchloride; In methanol; water; at 20 ℃;
DOI:10.1002/anie.202014108

Reference yield:

: 64884-78-2
4-methyl-N'-(nonan-5-ylidene)benzenesulfonohydrazide

: 111-84-2
nonane

Guidance literature:: With tetrahydrogenoboratebis(triphenylphosphine)copper(I); In chloroform; for 2h; Heating;
DOI:10.1016/S0040-4039(00)92863-6

Reference yield:

: 64884-78-2
4-methyl-N'-(nonan-5-ylidene)benzenesulfonohydrazide

: C₁₇H₂₆OS

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / toluene / 1 h / 20 °C / Inert atmosphere

1.2: 12 h / 100 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 0 °C / Inert atmosphere; Schlenk technique

2.2: 0.5 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2.3: 12 h / 60 °C / Inert atmosphere; Sealed tube

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/acs.orglett.8b03560