2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

Base Information

Chemical Name:2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide
CAS No.:336192-97-3
Molecular Formula:C₂₆H₂₅NO₂S
Molecular Weight:415.556
Hs Code.:

Synonyms:2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

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Chemical Property of 2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

Chemical Property:

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Technology Process of 2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

There total 1 articles about 2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 120363-13-5
tert-butyl 4-iodobenzoate

: 207724-47-8
2-(4-pyridinyl)ethyl-4'-(ethynyl)phenyl sulfide

: 336192-97-3
2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

Guidance literature:: With copper(l) iodide; diisopropylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; at 60 ℃;

Reference yield:

: 336192-97-3
2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

: 4-(4'-Hydroxycarbonylphenylethynyl)phenylthiol acetate

Guidance literature:: Multi-step reaction with 4 steps

1: acetone / 20 °C

2: aq. K₂CO₃ / dimethylformamide / 20 °C

3: 229 mg / imidazole / CH₂Cl₂ / 20 °C

4: 89 percent / aq. TFA / acetonitrile / 20 °C

With 1H-imidazole; potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 336192-97-3
2-(4'-Pyridyl)ethyl-[4''-(4'''-tert-butoxycarbonylphenyl)ethynyl]phenyl sulfide

: 336193-01-2
4-(4-mercapto-phenylethynyl)-benzoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 20 °C

2: aq. K₂CO₃ / dimethylformamide / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide; acetone;