ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Base Information

Chemical Name:ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4
CAS No.:130327-27-4
Molecular Formula:C₉H₂₁Cl₂N₃ORe*C₂₄H₂₀B
Molecular Weight:763.632
Hs Code.:

ReOCl<sub>2</sub>((CH<sub>3</sub>)NCH<sub>2</sub>CH<sub>2</sub>)3<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>={ReOCl<sub>2</sub>((CH<sub>3</sub>)NCH<sub>2</sub>CH<sub>2</sub>)3}B(C<sub>6</sub>H<sub>5</sub>)4

Synonyms:ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

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Chemical Property of ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

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Technology Process of ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

There total 2 articles about ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130327-30-9
Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

: 130327-27-4
ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Guidance literature:: With dimethyl sulfoxide; In dimethyl sulfoxide; byproducts: OP(C6H5)3, (CH3)2S; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.;

Reference yield:

: 130327-36-5
Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

: 130327-28-5
fac-[ReO₃(1,4,7-triazacyclononane)][BPh₄]

: 130327-27-4
ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Guidance literature:: In not given; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; 3 w; not isolated, monitored by NMR;

Reference yield: 85.0%

: 130327-27-4
ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

: 594-09-2
trimethylphosphane

: 130327-32-1
Re(OP(CH₃)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(CH₃)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Guidance literature:: In acetonitrile; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; addn. of phosphine to Re-complex in CH3CN, soln. stirred (15 min); evapn. (to 2-3 ml), addn. of Et2O, pptn., filtration, washed (Et2O), evapn., recrystn. from CH3CN; elem. anal.;