methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

Base Information

Chemical Name:methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate
CAS No.:1260170-97-5
Molecular Formula:C₁₈H₂₉N₃O₇S₂
Molecular Weight:463.576
Hs Code.:

Synonyms:methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

Suppliers and Price of methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

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Technology Process of methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

There total 9 articles about methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1260170-90-8
methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-(4-methanesulfonylpiperazin-1-yl)propanoate

: 106-94-5
propyl bromide

: 1260170-97-5
methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

Guidance literature:: With caesium carbonate; potassium iodide; In acetone; at 20 ℃; for 18h;

Reference yield: 50.0%

: 1260170-97-5
methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

Guidance literature:

Reference yield:

: 111712-04-0
4-phenylmethoxybenzenesulfonic acid sodium salt

: 1260170-97-5
methyl (S)-2-(4-methanesulfonylpiperazin-1-yl)-3-(4-propoxybenzenesulfonylamino)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

3: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol; 1,4-dioxane / 18 h / 20 °C / Inert atmosphere

4: caesium carbonate; potassium iodide / acetone / 18 h / 20 °C

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; caesium carbonate; acetic acid; triethylamine; potassium iodide; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;