10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

Base Information

Chemical Name:10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione
CAS No.:114113-38-1
Molecular Formula:C₂₄H₁₇N₃O₄S
Molecular Weight:443.483
Hs Code.:

Synonyms:10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

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Chemical Property of 10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

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Technology Process of 10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

There total 3 articles about 10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 114113-31-4,114113-32-5
(Z/E)-1-(4-Methylphenyl)-4-<(3-nitrophenyl)methylen>-pyrrolidin-2,3,5-trion

: 137-07-5
2-amino-benzenethiol

: 114113-38-1
10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

Guidance literature:: With hydrogenchloride; In ethanol; for 1h; Heating;
DOI:10.1055/s-1987-28130

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 114113-38-1
10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / conc. H₂SO₄ / acetic acid / 24 h / Ambient temperature

2: 94 percent / conc. HCl / ethanol / 1 h / Heating

With hydrogenchloride; sulfuric acid; In ethanol; acetic acid;
DOI:10.1055/s-1987-28130

Reference yield:

: 114113-26-7
N-(4-Methylphenyl)-2-hydroxy-maleinamidsaeuremethylester

: 114113-38-1
10-(3-Nitro-phenyl)-2-p-tolyl-4,10-dihydro-9-thia-2,4-diaza-benzo[f]azulene-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / conc. H₂SO₄ / acetic acid / 24 h / Ambient temperature

2: 94 percent / conc. HCl / ethanol / 1 h / Heating

With hydrogenchloride; sulfuric acid; In ethanol; acetic acid;
DOI:10.1055/s-1987-28130