1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

Base Information

Chemical Name:1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester
CAS No.:143747-61-9
Molecular Formula:C₂₂H₂₅Cl₂NO₃
Molecular Weight:422.351
Hs Code.:

1-<2-<bis(4-chlorophenyl)methoxy>ethyl>-3-piperidinecarboxylic acid methyl ester

Synonyms:1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

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Chemical Property of 1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

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Technology Process of 1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

There total 5 articles about 1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 110283-69-7
3-piperidinecarboxylic acid, 1-[2-[bis(4-chlorophenyl)methoxy]ethyl]-

: 143747-61-9
1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

Guidance literature:: In diethyl ether;
DOI:10.1021/jm00100a032

Reference yield:

: 90-97-1
4,4'-dichlorobenzophenone

: 143747-61-9
1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄ / toluene / 2 h / 85 - 90 °C

2: K₂CO₃ / acetonitrile / 15 h / Heating

3: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

4: 86 percent / diethyl ether

With lithium hydroxide; sulfuric acid; potassium carbonate; In methanol; diethyl ether; toluene; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 221916-05-8
1-bromo-2-[bis(4-chlorophenyl)methoxy]ethane

: 143747-61-9
1-<2-ethyl>-3-piperidinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

3: 86 percent / diethyl ether

With lithium hydroxide; potassium carbonate; In methanol; diethyl ether; acetonitrile;
DOI:10.1021/jm00100a032