(C₅H₅)2(C₅H₄CH(CH₃)C₆H₅)UCl

Base Information

• Chemical Name: (C₅H₅)2(C₅H₄CH(CH₃)C₆H₅)UCl
• CAS No.: 78790-03-1
• Molecular Formula: C₂₃H₂₃ClU
• Molecular Weight: 572.918
• Mol file: 78790-03-1.mol

Synonyms:(C₅H₅)2(C₅H₄CH(CH₃)C₆H₅)UCl

Chemical Property of (C₅H₅)2(C₅H₄CH(CH₃)C₆H₅)UCl

Chemical Property:

Purity/Quality:

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Technology Process of (C₅H₅)2(C₅H₄CH(CH₃)C₆H₅)UCl

There total 1 articles about (C₅H₅)2(C₅H₄CH(CH₃)C₆H₅)UCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

uranium(IV) chloride (10026-10-5) + (1-phenylethyl)cyclopentadienyllithium (78759-82-7) → tris(cyclopentadienyl)chlorouranium(IV) (1284-81-7) + (C5H5)2(C5H4CH(CH3)C6H5)UCl (78790-03-1)

Guidance literature:

In tetrahydrofuran; dropwise addition of equimolar amt. of cyclopentadienylide in THF to soln. of complex at -80°C, addition of 2 equiv. of cyclopentadienylsodium in THF, Ar atm.; evapn., extn. (heptane/toluene 1/1), crystn. at -80°C;

DOI:10.1016/S0022-328X(00)81191-2

upstream raw materials:

uranium(IV) chloride

(1-phenylethyl)cyclopentadienyllithium